%0 Book %T Polymer nucleation and crystallization investigated by in situ combination of atomic force microscopy (AFM) and fast scanning calorimetry (FSC) %A Zhang, Rui %D 2020 %C Rostock %C Universität Rostock %G English %F 1735636568 %O vorgelegt von Rui Zhang %O GutachterInnen: Rene Androsch (Martin Luther University Halle-Wittenberg, Interdisciplinary Center for Transfer-oriented Research in Natural Sciences) ; Christoph Schick (University of Rostock, Institution of Physics & Competence Centre CALOR) %O Dissertation Universität Rostock 2020 %X A chip based fast scanning calorimeter (FSC) is used as a fast hot-stage in an atomic force microscope (AFM). This way, the morphology of materials with a resolution from micro to nano meters after fast thermal treatments becomes accessible. FSC provides crystallization/melting curves of the sample just imaged by AFM. A combined AFM-FSC device is described, where the AFM sample holder is replaced by the FSC chip-sensor. The sample can be repeatedly annealed at pre-defined temperatures and times and the AFM images can be taken from exactly the same spot of the sample. %L 530 %9 theses %9 Text %9 Hochschulschrift %R 10.18453/rosdok_id00002777 %U http://purl.uni-rostock.de/rosdok/id00002777 %U https://nbn-resolving.org/urn:nbn:de:gbv:28-rosdok_id00002777-9 %U https://d-nb.info/1293660973/34 %U https://doi.org/10.18453/rosdok_id00002777